Distillation in Modern Chemistry Laboratory - How to Go About It?

In simple terminology, distillation is defined as theseparated, when there is a careful distillation of the
method of purifying a liquid by boiling it andmixture.
condensing its vapors. In other words, any liquidThis point is actually the temperature at which there
when it is heated and becomes fully boiled, theis an equality of vapor pressure of the liquid phase of
process of distillation captures and cools the resultanta compound to the external pressure working on the
hot vapors, and collect the condensed vapors. Thisliquid's surface. This outside pressure is usually the
method or process is not a chemical reaction but aatmospheric pressure. Let us explain this with an
unit operation or physical separation. In a modernexample:
chemistry laboratory, distillation is a very importantLet us consider a liquid in an open flask. The liquid is
requirement to identify and purify the organicheated. The vapor pressure of the liquid will increase
compounds.where there is an increase in the temperature of the
Boiling Point Determinationliquid. The liquid will boil when the vapor pressure is
The chemistry teaching labs make use of distillationequal to the atmospheric pressure. It is known that
regularly, for two purpose: identification of organicdifferent compounds boil at different temperatures
compounds and the purification of organicbecause each compound has its own vapor pressure.
compounds.It is to be noted that compounds with higher vapor
The boiling point of a compound implies the physicalpressures will boil at lower temperatures.
features or properties of a compound by which it isThe distillation process of determining a boiling point
distinguished. In a laboratory, distillation is used tomeasures the temperature of the vapors above the
purify a compound. This is done by separating theliquid and these vapors are the same temperature as
compound from less-volatile or a non-volatile material.the boiling liquid. If the boiling point is used to find a
There are different compounds in different points insolid compound, it is necessary to compare this with
a mixture and the individual components arethat of the true compound.